ISO 13163:2021 pdf download – Water quality — Lead-210 — Test method using liquid scintillation counting.
1 Scope This document specifies a method for the measurement of scintillation counting (LSC). 210 in all types of waters by liquid The method is applicable to test samples of supply/drinking water, rainwater, surface and ground water, as well as cooling water, industrial water, domestic, and industrial wastewater after proper sampling and handling, and test sample preparation. Filtration of the test sample is necessary. Lead-210 activity concentration in the environment can vary and usually ranges from 2 mBq l to 300 mBq l . Using currently available liquid scintillation counters, the limit of detection of this method for Pb is generally of the order of 20 mBq l to 50 mBq l , which is lower than the WHO criteria for safe consumption of drinking water (100 mBq l ). These values can be achieved with a counting time between 180 min and 720 min for a sample volume from 0,5 l to 1,5 l. Higher activity concentrations can be measured by either diluting the sample or using smaller sample aliquots or both. The method presented in this document is not intended for the determination of an ultra-trace amount of Pb. The range of application depends on the amount of dissolved material in the water and on the performance characteristics of the measurement equipment (background count rate and counting efficiency). The method described in this document is applicable to an emergency situation. The analysis of Pb adsorbed to suspended matter is not covered by this method. It is the user ’s responsibility to ensure the validity of this test method for the water samples tested. 2 Normative references The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO/IEC Guide 98-3, Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) ISO/IEC Guide 99, International vocabulary of metrology — Basic and general concepts and associated terms (VIM) ISO 3696, Water for analytical laboratory use — Specification and test methods ISO 5667-1, Water quality — Sampling — Part 1: Guidance on the design of sampling programmes and sampling techniques ISO 5667-3, Water quality — Sampling — Part 3: Preservation and handling of water samples
ISO 5667-10, Water quality — Sampling — Part 10: Guidance on sampling of waste water ISO 11929 (all parts), Determination of the characteristic limits (decision threshold, detection limit and limits of the coverage interval) for measurements of ionizing radiation — Fundamentals and application ISO/IEC 17025, General requirements for the competence of testing and calibration laboratories ISO 19361, Measurement of radioactivity — Determination of beta emitters activities — Test method using liquid scintillation counting ISO 80000-10, Quantities and units — Part 10: Atomic and nuclear physics
ISO 13163:2021 pdf download – Water quality — Lead-210 — Test method using liquid scintillation counting
